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Through Thin Film Ablation of Iron-Nickel Pixel Target

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2010, Master of Science (M.S.), University of Dayton, Materials Engineering.
A novel multi-element nanoparticle synthesis technique, noted pixel target ablation (PTA) is reported here. In the experiments described here, Iron-Nickel pixel targets were prepared on a transparent disc by sputtering and by photolithography. By irradiating the target materials from the backside, the laser energy breaks the target materials into metal atoms, which then forms nanoparticles by recombination in the gas phase. The nanoparticles were subsequently captured by a substrate. The degree of interaction between the two metals species and the plume dynamics of this method were examined. The average composition and size distribution of synthesized nanoparticles were studied using X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy (TEM) respectively. The results show that this process has congruent transformation of target materials weight ratio to particle composition, and controllable particle size distribution with no agglomeration. Additionally, the structure of the particles was determined by the use of X-ray diffraction (XRD). Samples were prepared by ablation in vacuum and in the presence of a background gas. A mixture of single-metallic and alloyed nanoparticles were collected. The implications of these observations for multi-element nanoparticle synthesis are discussed.
Paul Murray, PhD (Committee Chair)
Daniel Eylon (Committee Member)
Andrew Sarangan (Committee Member)
56 p.

Recommended Citations

Citations

  • Niu, X. (2010). Through Thin Film Ablation of Iron-Nickel Pixel Target [Master's thesis, University of Dayton]. OhioLINK Electronic Theses and Dissertations Center. http://rave.ohiolink.edu/etdc/view?acc_num=dayton1280153225

    APA Style (7th edition)

  • Niu, Xiaoxu. Through Thin Film Ablation of Iron-Nickel Pixel Target. 2010. University of Dayton, Master's thesis. OhioLINK Electronic Theses and Dissertations Center, http://rave.ohiolink.edu/etdc/view?acc_num=dayton1280153225.

    MLA Style (8th edition)

  • Niu, Xiaoxu. "Through Thin Film Ablation of Iron-Nickel Pixel Target." Master's thesis, University of Dayton, 2010. http://rave.ohiolink.edu/etdc/view?acc_num=dayton1280153225

    Chicago Manual of Style (17th edition)