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Design and Performance of Macroscopic and Microscopic Prism-based Infrared Spectrographs Using Focal Plane Array Detectors

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2010, Doctor of Philosophy, Miami University, Chemistry and Biochemistry.
Planar array infrared (PA-IR) spectroscopy has recently been employed as an alternative to Fourier transform infrared (FT-IR) spectroscopy for studies involving dynamic chemical events. At the onset of this thesis, most PA-IR instruments were grating-based, which typically provided a sufficient spectral resolution but a poor spectral coverage. The results of this thesis demonstrated that prism-based spectrographs can be viable alternatives to grating-based spectrographs when spectral coverage is more important than spectral resolution. Chapter 1 serves as an introduction into FT-IR and PA-IR spectroscopy. Chapter 2 focused on the development of macroscopic transmission prism-based spectrographs, Chapter 3 evaluated the performance of an attenuated total internal reflection (ATR)-PA-IR spectrograph, Chapter 4 investigated the potential for PA-IR microspectroscopy and Chapter 5 employed ATR-PA-IR spectroscopy as a detection technique for liquid chromatography. Chapter 6 deviates slightly from the rest of this thesis and involved comparing macro ATR-FT-IR and micro ATR-FT-IR imaging for the analysis of counterfeit pharmaceutical tablets.
Andre Sommer, PhD (Advisor)
Neil Danielson, PhD (Committee Chair)
Curtis Marcott, PhD (Committee Member)
Shouzhong Zou, PhD (Committee Member)
Lei Kerr, PhD (Committee Member)
181 p.

Recommended Citations

Citations

  • Lanzarotta, A. C. (2010). Design and Performance of Macroscopic and Microscopic Prism-based Infrared Spectrographs Using Focal Plane Array Detectors [Doctoral dissertation, Miami University]. OhioLINK Electronic Theses and Dissertations Center. http://rave.ohiolink.edu/etdc/view?acc_num=miami1272740376

    APA Style (7th edition)

  • Lanzarotta, Adam. Design and Performance of Macroscopic and Microscopic Prism-based Infrared Spectrographs Using Focal Plane Array Detectors. 2010. Miami University, Doctoral dissertation. OhioLINK Electronic Theses and Dissertations Center, http://rave.ohiolink.edu/etdc/view?acc_num=miami1272740376.

    MLA Style (8th edition)

  • Lanzarotta, Adam. "Design and Performance of Macroscopic and Microscopic Prism-based Infrared Spectrographs Using Focal Plane Array Detectors." Doctoral dissertation, Miami University, 2010. http://rave.ohiolink.edu/etdc/view?acc_num=miami1272740376

    Chicago Manual of Style (17th edition)