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Investigating Heterogeneous Nucleation of Barite using Hydrothermal Atomic Force Microscopy and Optical Microscopy.

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2020, Master of Science (MS), Wright State University, Chemistry.
In order to develop a better understanding heterogeneous nucleation of barite, barite precipitation was studied under varying experimental parameters. Hydrothermal atomic force microscopy (HAFM) and optical microscopy were used to investigate the effect of change in temperature, supersaturation and varying ratios of ions on heterogeneous nucleation of barite. In the experiments conducted at higher temperatures, the particles thus nucleated were found to display characteristic hexagonal and rhomboidal shapes. In comparing results of particle densities among different ion ratios, there is evidence suggesting that barium to sulfate ratio plays a role of promoter. Wherein, the ratios with higher [Ba2+] concentration were found to show more nucleation occurring. Although, the HAFM cell was used for experimentation, optical microscopy turned out to be a more effective method for analysis of samples.
Steven Higgins, Ph.D. (Advisor)
David Dolson, Ph.D. (Committee Member)
Ioana Pavel, Ph.D. (Committee Member)
58 p.

Recommended Citations

Citations

  • Gurav, A. B. (2020). Investigating Heterogeneous Nucleation of Barite using Hydrothermal Atomic Force Microscopy and Optical Microscopy. [Master's thesis, Wright State University]. OhioLINK Electronic Theses and Dissertations Center. http://rave.ohiolink.edu/etdc/view?acc_num=wright1610403323603442

    APA Style (7th edition)

  • Gurav, Ankita. Investigating Heterogeneous Nucleation of Barite using Hydrothermal Atomic Force Microscopy and Optical Microscopy. 2020. Wright State University, Master's thesis. OhioLINK Electronic Theses and Dissertations Center, http://rave.ohiolink.edu/etdc/view?acc_num=wright1610403323603442.

    MLA Style (8th edition)

  • Gurav, Ankita. "Investigating Heterogeneous Nucleation of Barite using Hydrothermal Atomic Force Microscopy and Optical Microscopy." Master's thesis, Wright State University, 2020. http://rave.ohiolink.edu/etdc/view?acc_num=wright1610403323603442

    Chicago Manual of Style (17th edition)