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Synthesis of bis(2,2,2-trifluoroethyl) β-ketophosphonates from bis(2,2,2-trifluoroethyl) 1-alkynylphosphonates via enamine vinyl phosphonates

DePizzo, Ashley

Abstract Details

2010, Master of Science in Chemistry, Youngstown State University, Department of Chemistry.
A new method for the synthesis of bis(2,2,2-trifluoroethyl) β-ketophosphonates from bis(2,2,2-trifluoroethyl) 1-alkynylphosphonates is described herein. Bis(2,2,2-trifluoroethyl) 1-alkynylphosphonates can be treated with primary and secondary amines to prepare enamine vinyl phosphonates. Bis(2,2,2-trifluoroethyl) β-ketophosphonates are obtained after hydrolysis of the enamine vinyl phosphonate.
John Jackson, PhD (Advisor)
Peter Norris, PhD (Committee Member)
Michael Serra, PhD (Committee Member)
64 p.

Recommended Citations

Citations

  • DePizzo, A. (2010). Synthesis of bis(2,2,2-trifluoroethyl) β-ketophosphonates from bis(2,2,2-trifluoroethyl) 1-alkynylphosphonates via enamine vinyl phosphonates [Master's thesis, Youngstown State University]. OhioLINK Electronic Theses and Dissertations Center. http://rave.ohiolink.edu/etdc/view?acc_num=ysu1287586787

    APA Style (7th edition)

  • DePizzo, Ashley. Synthesis of bis(2,2,2-trifluoroethyl) β-ketophosphonates from bis(2,2,2-trifluoroethyl) 1-alkynylphosphonates via enamine vinyl phosphonates. 2010. Youngstown State University, Master's thesis. OhioLINK Electronic Theses and Dissertations Center, http://rave.ohiolink.edu/etdc/view?acc_num=ysu1287586787.

    MLA Style (8th edition)

  • DePizzo, Ashley. "Synthesis of bis(2,2,2-trifluoroethyl) β-ketophosphonates from bis(2,2,2-trifluoroethyl) 1-alkynylphosphonates via enamine vinyl phosphonates." Master's thesis, Youngstown State University, 2010. http://rave.ohiolink.edu/etdc/view?acc_num=ysu1287586787

    Chicago Manual of Style (17th edition)