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ysu997203540.pdf (1.08 MB)
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Synthesis of BIS(2.2,2-Trifluoroethyl) vinylphosphates
Author Info
Stock, Joseph R.
Permalink:
http://rave.ohiolink.edu/etdc/view?acc_num=ysu997203540
Abstract Details
Year and Degree
1998, Master of Science in Chemistry, Youngstown State University, Department of Chemistry.
Abstract
The focus of the research presented here is the synthesis, isolation and characterization of vinyl phosphates containing the bis(2,2,2-trifluorethyl) group. The first step involved the synthesis of bis(2,2,2-trifluoroethoxy) phosphorochloridate. This reagent was then added to a ketone enolate, formed by the reaction of LDA, prepared in situ from diisopropylamine and η-butyllithium, and a cyclic ketone to yield the desired vinyl phosphates.
Committee
John Jackson (Advisor)
Pages
74 p.
Keywords
vinyl phosphates
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Citations
Stock, J. R. (1998).
Synthesis of BIS(2.2,2-Trifluoroethyl) vinylphosphates
[Master's thesis, Youngstown State University]. OhioLINK Electronic Theses and Dissertations Center. http://rave.ohiolink.edu/etdc/view?acc_num=ysu997203540
APA Style (7th edition)
Stock, Joseph.
Synthesis of BIS(2.2,2-Trifluoroethyl) vinylphosphates.
1998. Youngstown State University, Master's thesis.
OhioLINK Electronic Theses and Dissertations Center
, http://rave.ohiolink.edu/etdc/view?acc_num=ysu997203540.
MLA Style (8th edition)
Stock, Joseph. "Synthesis of BIS(2.2,2-Trifluoroethyl) vinylphosphates." Master's thesis, Youngstown State University, 1998. http://rave.ohiolink.edu/etdc/view?acc_num=ysu997203540
Chicago Manual of Style (17th edition)
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Document number:
ysu997203540
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Copyright Info
© 1998, all rights reserved.
This open access ETD is published by Youngstown State University and OhioLINK.