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Debora Daloia 6-20-2014 with copyright page final format approved LW 6-23-14 (2).pdf (3.38 MB)
ETD Abstract Container
Abstract Header
Friction and Wear Behavior of Graphene Reinforced Epoxy
Author Info
Daloia, Debora
Permalink:
http://rave.ohiolink.edu/etdc/view?acc_num=dayton1403532384
Abstract Details
Year and Degree
2014, Master of Science (M.S.), University of Dayton, Materials Engineering.
Abstract
The focus of this study was to investigate the effect of graphene content on physical, mechanical, and tribological behavior of epoxy resin. Four composite samples, consisting of 0, 1%, 5%, and 10wt% graphene were fabricated using a 3 roll mill for dispersion and heat press for curing. Friction and wear tests were conducted on a laboratory scale tribo-test dynamometer, using a ring-on-flat configuration, for one hour duration at an average sliding speed of 0.3 m/s under a variable pressure of 0.26 to 0.39 MPa. Dynamic mechanical analysis (DMA) was used to determine the storage and loss moduli and contact angle measurements were determined to compute the surface energy of worn and unworn composite samples. Scanning electron microscopy and polarized light microscopy was used to study the graphene dispersion in the epoxy and study the wear mechanisms. In addition, electrical conductivity was measured to determine the percolation threshold and as an alternate method to verify the graphene dispersion in the epoxy. The tests indicate that storage modulus and surface energy increased by 62.5% and 55% respectively with graphene content. The tribological behavior of graphene composites showed that this nanofiller was very effective in stabilizing the coefficient of friction and reducing wear rate as well. Neat epoxy showed a high wear rate and an unstable coefficient of friction. On the other hand, 5wt% of graphene exhibited the highest stable coefficient of friction. The improvement on wear resistance was remarkable, for example, the 10wt% composite resulted in a wear reduction of almost 98% when compared with the neat epoxy. It may be noted that the manufacture of graphene based composites was relatively easy, quick, and inexpensive while the samples exhibited improvements in many relevant properties.
Committee
Khalid Lafdi, Ph.D (Committee Chair)
Vinod Jain, Ph.D (Committee Member)
Klosterman Donald, Ph.D (Committee Member)
Pages
101 p.
Subject Headings
Chemical Engineering
;
Materials Science
;
Mechanical Engineering
;
Nanoscience
;
Nanotechnology
Keywords
Friction
;
Wear
;
Graphene
;
Reinforced
;
Epoxy
;
polymer
;
tribology
;
tribological
;
nanofiller
;
nanomaterial
;
composite
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Citations
Daloia, D. (2014).
Friction and Wear Behavior of Graphene Reinforced Epoxy
[Master's thesis, University of Dayton]. OhioLINK Electronic Theses and Dissertations Center. http://rave.ohiolink.edu/etdc/view?acc_num=dayton1403532384
APA Style (7th edition)
Daloia, Debora.
Friction and Wear Behavior of Graphene Reinforced Epoxy.
2014. University of Dayton, Master's thesis.
OhioLINK Electronic Theses and Dissertations Center
, http://rave.ohiolink.edu/etdc/view?acc_num=dayton1403532384.
MLA Style (8th edition)
Daloia, Debora. "Friction and Wear Behavior of Graphene Reinforced Epoxy." Master's thesis, University of Dayton, 2014. http://rave.ohiolink.edu/etdc/view?acc_num=dayton1403532384
Chicago Manual of Style (17th edition)
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Document number:
dayton1403532384
Download Count:
6,690
Copyright Info
© 2014, all rights reserved.
This open access ETD is published by University of Dayton and OhioLINK.