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ysu1230924488.pdf (2.06 MB)
ETD Abstract Container
Abstract Header
Quantitation of Halogenated Anisoles in Wine via SPME – GC/MS
Author Info
Milo, John A.
Permalink:
http://rave.ohiolink.edu/etdc/view?acc_num=ysu1230924488
Abstract Details
Year and Degree
2008, Master of Science in Chemistry, Youngstown State University, Department of Chemistry.
Abstract
This research study involves the development and optimization of solid-phase microextraction (SPME) coupled with gas chromatography-mass spectrometry (GC-MS) for the analysis of halogenated anisoles present in wines at ultra-trace amounts. The presence of these compounds in wines unfortunately affects the aroma, ruins the overall taste, and accounts for huge monetary losses in the wine industry every year. The work described herein focuses on the quantitation of these undesirable compounds at levels below olfactory threshold limits and the development and validation of the extraction procedure method associated with SPME. Multiple commercial wine samples, contaminated with these unwanted compounds, were analyzed where the actual amount of halogenated anisoles was determined.
Committee
Brian Leskiw, PhD (Advisor)
Roland Riesen, PhD (Committee Member)
Larry Curtin, PhD (Committee Member)
Pages
81 p.
Subject Headings
Chemistry
Keywords
solid-phase microextraction
;
haloanisoles
;
gas chromatography mass spectrometry
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Citations
Milo, J. A. (2008).
Quantitation of Halogenated Anisoles in Wine via SPME – GC/MS
[Master's thesis, Youngstown State University]. OhioLINK Electronic Theses and Dissertations Center. http://rave.ohiolink.edu/etdc/view?acc_num=ysu1230924488
APA Style (7th edition)
Milo, John.
Quantitation of Halogenated Anisoles in Wine via SPME – GC/MS.
2008. Youngstown State University, Master's thesis.
OhioLINK Electronic Theses and Dissertations Center
, http://rave.ohiolink.edu/etdc/view?acc_num=ysu1230924488.
MLA Style (8th edition)
Milo, John. "Quantitation of Halogenated Anisoles in Wine via SPME – GC/MS." Master's thesis, Youngstown State University, 2008. http://rave.ohiolink.edu/etdc/view?acc_num=ysu1230924488
Chicago Manual of Style (17th edition)
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Document number:
ysu1230924488
Download Count:
875
Copyright Info
© 2008, all rights reserved.
This open access ETD is published by Youngstown State University and OhioLINK.